Green Synthesis of Magnetic Nanoparticles of Iron Oxide Using Aqueous Extracts of Lemon Peel Waste and Its Application in Anti-Corrosive Coatings

Elizondo Villarreal, Nora y Verástegui Domínguez, Luz Hypatia y Rodríguez Batista, Raúl y Gándara Martínez, Eleazar y Alcorta García, Aracelia y Martínez Delgado, Dora Irma y Rodríguez Castellanos, Edén Amaral y Vázquez Rodríguez, Francisco Javier y Gómez Rodríguez, Cristian (2022) Green Synthesis of Magnetic Nanoparticles of Iron Oxide Using Aqueous Extracts of Lemon Peel Waste and Its Application in Anti-Corrosive Coatings. Materials, 15 (23). pp. 1-22. ISSN 1996-1944

Vista previa

Texto
26210.pdf - Versión Publicada
Available under License Creative Commons Attribution Non-commercial No Derivatives.
Download (5MB) | Vista previa

URL o página oficial: http://doi.org/10.3390/ma15238328

Resumen

Lately, the development of green chemistry methods with high efficiency for metal nanoparticle synthesis has become a primary focus among researchers. The main goal is to find an eco-friendly technique for the production of nanoparticles. Ferro- and ferrimagnetic materials such as magnetite (Fe3O4) exhibit superparamagnetic behavior at a nanometric scale. Magnetic nanoparticles have been gaining increasing interest in nanoscience and nanotechnology. This interest is attributed to their physicochemical properties, particle size, and low toxicity. The present work aims to synthesize magnetite nanoparticles in a single step using extracts of green lemon Citrus Aurantifolia residues. The results produced nanoparticles of smaller size using a method that is friendlier to health and the environment, is more profitable, and can be applied in anticorrosive coatings. The green synthesis was carried out by a co-precipitation method under variable temperature conditions. The X-ray Diffraction (XRD) and Transmission Electron Microscopy (TEM) characterization showed that magnetite nanoparticles were successfully obtained with a very narrow particle size distribution between 3 and 10 nm. A composite was produced with the nanoparticles and graphene to be used as a surface coating on steel. In addition, the coating’s anticorrosive behavior was evaluated through electrochemical techniques. The surface coating obtained showed good anticorrosive properties and resistance to abrasion.

Tipo de elemento:

Article

Palabras claves no controlados:

Nanopartículas de magnetita; Síntesis verde; Extractos de cáscara de limón; Revestimientos anticorrosivos; Método ecológico

Materias:

T Tecnología > TA Ingeniería General y Civil

Divisiones:

Ciencias Físico Matemáticas

Usuario depositante:

Editor Repositorio

Creadores:

Creador	Email	ORCID
Elizondo Villarreal, Nora	NO ESPECIFICADO	orcid.org/0000-0002-1661-7756
Verástegui Domínguez, Luz Hypatia	NO ESPECIFICADO	NO ESPECIFICADO
Rodríguez Batista, Raúl	NO ESPECIFICADO	NO ESPECIFICADO
Gándara Martínez, Eleazar	NO ESPECIFICADO	NO ESPECIFICADO
Alcorta García, Aracelia	NO ESPECIFICADO	NO ESPECIFICADO
Martínez Delgado, Dora Irma	NO ESPECIFICADO	orcid.org/0000-0003-1665-209X
Rodríguez Castellanos, Edén Amaral	NO ESPECIFICADO	NO ESPECIFICADO
Vázquez Rodríguez, Francisco Javier	francisco.vazquezrd@outlook.es	orcid.org/0000-0001-5010-9491
Gómez Rodríguez, Cristian	NO ESPECIFICADO	NO ESPECIFICADO